The Practical Distiller An Introduction To Making Whiskey, Gin, Brandy, Spirits, &c. &c. of Better Quality, and in Larger Quantities, than Produced by the Present Mode of Distilling, from the Produce of the United States

Part 3

Chapter 34,309 wordsPublic domain

Distillers will doubtless make experiments of the various modes recommended and use that which may prove most advantageous and convenient.

ART. III.

_To Mash two thirds Rye and one third Corn in Summer._

This I have found to be the nicest process belonging to distilling--the small proportion of corn, and the large quantity of scalding water, together with the easy scalding of rye, and the difficulty of scalding corn, makes it no easy matter to exactly hit the scald of both; but as some distillers continue to practice it, (altho' not a good method in my mind, owing to the extreme nice attention necessary in performing it.) In the following receipt I offer the best mode within my knowledge, and which I deem the most beneficial, and in which I shew the process and mode pursued by other distillers.

Take four gallons cold water, put it into a hogshead, then stir half a bushel corn into it, let it stand uncovered thirty minutes, then add sixteen gallons boiling water, stir it well, cover it close for fifteen minutes, then put in your rye and malt and stir it until there be no lumps, then cover it and stir it at intervals until your still boils, then add, eight, twelve, or sixteen gallons boiling water, or such quantity as you find from experience, to answer best--(but with most water, twelve gallons will be found to answer) stirring it well every fifteen minutes until you perceive it is scalded enough, then uncover and stir it effectually until you cool off; keeping in mind always that the more effectually you stir it, the more whiskey will be yielded. This method I have found to answer best, however, I have known it to do very well, by soaking the corn in the first place, with two gallons warm, and two gallons cold water, instead of the four gallons of cold water, mentioned above--others put in the rye, when all the boiling water is in the hogshead, but I never found it to answer a good purpose, nor indeed did I ever find much profit in distilling rye and corn in this proportion.

ART. IV.

_To distill one half Rye and one half Corn._

This method of distilling equal quantities of rye and corn, is more in practice, and is much better than to distill unequal proportions, for reason you can scald your corn and rye to a certainty, and the produce is equal if not more, and better whiskey, than all rye. The indian corn is cheaper, and the seed is better than if all rye. I would recommend this, as the smallest quantity of corn to be mixed with rye for distillation, as being most productive, and profitable. The following receipt I have found to answer all waters--yet there may be places where the distiller cannot follow this receipt exactly, owing to hard or soft water, (as it is generally termed) or hard flint or soft floury corn, that will either scald too much or too little--but this the attentive distiller will soon determine by experience.

Have your hogshead perfectly sweet, put into each, three gallons of cold and three of boiling water, or more or less of each, as you find will answer best--then stir in your corn--fill up your boiler, bring it briskly to a boil--then put to each hogshead twelve gallons boiling water, giving each hogshead one hundred stirs, with your mashing stick, then cover close, fill up your boiler and keep a good fire under her, to produce a speedy boil; before you add the last water, put into each hogshead one pint of salt, and a shovel full of hot coals and ashes from under your still, stir the salt and coals well, to mix it with your corn, the coal will remove any bad smell which may be in the hogshead--Should you find on trial, that rye don't scald enough, by putting it in after your last water, you may in that case put in your rye before the last water--but this should be ascertained from several experiments. I have found it to answer best to put in the rye after all the water is in the hogshead, especially if you always bring the still briskly to a boil--then on your corn put twelve or sixteen gallons boiling water, (for the last water,) then if you have not already mashed in your rye, put it in with one gallon good malt to each hogshead, carefully stirring it immediately very briskly, for fear of the water loosing its heat, and until the lumps are all broken, which you will discover by looking at your mashing stick; lumps generally stick to it. When done stirring, cover the hogshead close for half an hour, then stir it to ascertain whether your grain be sufficiently scalded, and when nearly scalded enough, uncover and stir steady until you have it cool enough to stop scalding; when you see it is scalded enough, and by stirring that the scalding is stopped, uncover your hogsheads, and stir them effectually, every fifteen minutes, until they are fit to cool off--remembering that sweet good yeast, clean sweet hogsheads, with this mode of mashing carefully, will produce you a good turn out of your grain. The quantity of corn and rye is generally two stroked half bushels of each, and one gallon malt.

ART. V.

_To Mash one third Rye and two thirds Corn._

This I deem the most profitable mashing that a distiller can work, and if he can get completely in the way of working corn and rye in this proportion, he will find it the easiest process of mashing. That corn has as much and as good whiskey as rye or any other grain, cannot be disputed, and the slop or pot ale is much superior to that of any other grain, for feeding or fattening either horned cattle or hogs--one gallon of corn pot ale being esteemed worth three of rye, and cattle will always eat it better--and moreover, corn is always from one to two shillings per bushel cheaper than rye, and in many places much plentier--so that by adopting this method and performing it well, the distiller will find at the close of the year, it has advantages over all other processes and mixtures of rye and corn, yielding more profit, and sustaining the flock better. Hogs fatted on this pot ale, will be found decidedly better than any fatted on the slops of any other kind of mashing.

_Mash as follows._

Have sweet hogsheads, good yeast and clean water in your boiler; when the water is sharp, warm, or half boiling, put into every hogshead you mean to mash at the same time, six, eight or as many gallons of the half boiling water, as will completely wet one bushel corn meal--add then one bushel chopped corn, stir it with your mashing stick till your corn is all wet; it is better to put in a less quantity of water first, and so add as you may find necessary, until completely wet (be careful in all mashings, that your mashing stick be clean), this is called soaking the corn. Then fill up your boiler, bring her quickly to a boil, when effectually boiling, put into every hogshead, twelve gallons boiling water, stirring it well after putting in each bucket, until the lumps are quite broken--cover the hogsheads close, after a complete stirring--fill up your boiler, bring her quickly to boil for the last mashing--stir the corn in the hogshead every fifteen minutes, till your last water is boiling--put into each hogshead one pint salt, and a shovel full of red hot coals, stirring it well--then put in each hogshead sixteen gallons of boiling water, stir it well--cover it close for twenty-five minutes--then put into each hogshead one half bushel rye meal, and one gallon good chopped malt, stirring it until the lumps are all broken, then cover it close, stir it every half hour, until you perceive it sufficiently scalded--then uncover it and stir it as often as your other business will permit, until ready to cool off.

In this and every other mashing you must use sweet vessels only and good yeast, or your labor will be in vain; and in all kinds of mashing you cannot stir too much.

ART. VI.

_To Mash Corn._

This is an unprofitable and unproductive mode of mashing, but there may be some times when the distiller is out of rye, on account of the mill being stopped, bad roads, bad weather, or some other cause; and to avoid the necessity of feeding raw grain to the hogs or cattle, (presuming every distillery to be depended on for supplying a stock of some kind, and often as a great reliance for a large stock of cattle and hogs,) in cold weather I have found it answer very well, but in warm weather it will not do. Those who may be compelled then from the above causes, or led to it by fancy, may try the following method. To one hogshead, put twelve gallons boiling water, and one and an half bushels corn, stir it well, then when your water boils, add twelve gallons more, (boiling hot,) stir it well, and cover it close, until the still boils the third time, then put in each hogshead, one quart of salt, and sixteen gallons boiling water, stir it effectually, cover it close until you perceive it nearly scalded enough, then put in two, or three gallons cold water, (as you will find to answer best,) and two gallons malt, or more if it can be spared--stir it well, then cover it for half an hour, then uncover and stir it well, until cold enough to cool off.

ART. VII.

_To make four gallons from the bushel._

This is a method of mashing that I much approve of, and recommend to all whiskey distillers to try it--it is easy in process, and is very little more trouble than the common method, and may be done in every way of mashing, as well with corn or rye, as also a mixture of each, for eight months in the year; and for the other four is worth the trouble of following. I do not mean to say that the quantity of four gallons can be made at an average, in every distillery, with every sort of grain, and water, or during every vicissitude of weather, and by every distiller, but this far I will venture to say, that a still house that is kept in complete order, with good water, grain well chopped, good malt, hops, and above all good yeast; together with an apt, careful and industrious distiller, cannot fail to produce at an average for eight months in the year, three and three quarter gallons from the bushel at a moderate calculation. I have known it sometimes produce four and an half gallons to the bushel, for two or three days, and sometimes for as many weeks, when perhaps, the third or fourth day, or week, it would scarcely yield three gallons; a change we must account for, in a change of weather, the water or the neglect or ignorance of the distiller. For instance, we know that four gallons of whiskey is in the bushel of rye or corn--certain, that this quantity has been made from the bushel; then why not always? Because, is the answer, there is something wrong, sour yeast or hogsheads, neglect of duty in the distiller, change of grain, or change of weather--then of course it is the duty of the distiller to guard against all these causes as near as he can. The following method, if it does not produce in every distillery the quantity above mentioned, will certainly produce more whiskey from the bushel, than any other mode I have ever known pursued.

Mash your grain in the method that you find will yield you most whiskey--the day before you intend mashing, have a clean hogshead set in a convenient part of the distillery; when your singling still is run off, take the head off and fill her up with clean water, let her stand half an hour, to let the thick part settle to the bottom, which it will do when settled, dip out with a gallon or pail, and fill the clean hogshead half full, let the hogshead stand until it cools a little, so that when you fill it up with cool water, it will be about milk-warm, then yeast it off with the yeast for making 4 gallons to the bushel, then cover it close, and let it work or ferment until the day following, when you are going to cool off; when the cold water is running into your hogshead of mashed stuff, take the one third of this hogshead to every hogshead, (the above being calculated for three hogsheads) to be mashed every day, stirring the hogsheads well before you yeast them off. This process is simple, and I flatter myself will be found worthy of the trouble.

ART. VIII.

_To know when Grain is scalded enough._

Put your mashing stick into your hogshead and stir it round two or three times gently, then lift it out and give it a gentle stroke on the edge of your hogshead--if you perceive the batter or musky part fall off your stick, and there remains the heart of the grain on your mashing stick, like grains of timothy seed, then be assured that it is sufficiently scalded, if not too much, this hint will suffice to the new beginner, but experience and observation will enable the most correct judgment.

ART. IX.

_Directions for cooling off._

Much observation is necessary to enable the distiller to cool off with judgment--which necessity is increased by the versatility of our climate, the seasons of the year, and the kinds of water used. These circumstances prevent a strict adherence to any particular or specific mode; I however submit a few observations for the guidance of distillers in this branch.--If in summer you go to cool off with cold spring water, then of course the mashed stuff in your hogsheads must be much warmer, than if you intended cooling off with creek or river water, both of which are generally near milk warm, which is the proper heat for cooling off--In summer a little cooler, and in winter a little warmer.

It will be found that a hogshead of mashed grain will always get warmer, after it begins to work or ferment.

When the mashed stuff in your hogsheads is brought to a certain degree of heat, by stirring, which in summer will feel sharp warm, or so warm, that you can hardly bear your hand in it for any length of time, will do for common water, but for very cold or very warm water to cool off with, the stuff in the hogsheads must be left colder or warmer, as the distiller may think most expedient, or to best suit the cooling off water.

When you think it is time to cool off, have a trough or conveyance to bring the water to your hogsheads ready--let the hogsheads be well stirred, then let the water run into them slowly, stirring them all the time the water is running in, until they are milk warm, then stop the water, and after stirring them perfectly, put in the yeast and stir it until completely incorporated with the mashed stuff, then cover your hogshead until it begins to ferment or work, then uncover it.

ART. X.

_To ascertain when Rye works well in the Hogshead._

When mashed rye begins to work or ferment in the hogsheads, either in a heavy, thick, or light bubbly top, both of which are unfavorable; when it rises in a thick heavy top, you may be sure there is something wrong, either in the grain, yeast, or cooling off. When the top (as called by distillers) appear, with bubbles about the size of a nutmeg, rising and falling alternately, with the top not too thick nor too thin, and with the appearance of waves, mixed with the grain in the hogshead, rising and falling in succession, and when you put your head over the steam, and it flying into your nose, will have a suffocating effect, or when it will instantly extinguish a candle when held over it, you may feel assured, it is working well.

From these hints and the experience of the distiller, a judgment may be formed of the state of fermentation and the quality.

ART. XI.

_To prevent Hogsheads from working over._

If the stuff is cooled off too warm, or too much yeast is put in the hogsheads, they will work over, and of course lose a great deal of spirit, to prevent which, take tallow and rub round the chine of the hogsheads a little higher than they ought to work; it will generally prevent them from rising any higher, but if they will work over in spite of this remedy, then drop a little tallow into the stuff, it will immediately sink the stuff to a proper height.

SECTION IV.

ARTICLE I.

_Observations on the quality of Rye for distilling._

The best rye for distilling is that which is thoroughly ripe, before it is cut, and kept dry till threshed; if it has grown on high or hilly ground, it is therefore to be preferred, being then sounder and the grain fuller, than that produced on low level land--but very often the distiller has no choice, but must take that which is most convenient;--great care however ought to be observed in selecting sound rye, that has been kept dry, is clean and free from cockle, and all kind of dirt, advantages will result from fanning it, or running it through a windmill before it is chopped.

ART. II.

_Mode of chopping Rye and the proper size._

The mill stones ought to be burrs, and kept very sharp for chopping rye for distillation; and the miller ought to be careful not to draw more water on the wheel than just sufficient to do it well, and avoid feeding the stones plentifully; because in drawing a plentiful supply of water, the wheel will compel a too rapid movement of the stones, of course render it necessary they should be more abundantly fed, which causes part to be ground dead, or too fine, whilst part thereof will be too coarse, and not sufficiently broken, so that a difficulty arises in scalding--for in this state it will not scald equally, and of consequence, the fermentation cannot be so good or regular; and moreover as part of it will merely be flattened, a greater difficulty will arise in breaking the lumps, when you mash and stir your hogsheads. If burr stones are very sharp, I recommend the rye to be chopped very fine, but to guard against over-seeding, or pressing too much on them; but if the stones are not sharp, I would recommend the rye should be chopped about half fine. Distillers in general sustain a loss from having their rye chopped so coarse as I have observed it done in common.

ART. III.

_Chopping or Grinding Indian Corn._

Indian corn cannot be ground too fine for distilling.

ART. IV.

_Malt_

Cannot be ground too coarse, provided it is done even--there ought to be no fine nor coarse grains in malt, but ground perfectly alike, and of the same grade. If ground too fine, it will be apt to be scalded too much in mashing. Malt does not require half the scalding necessary in rye. Let the distiller try the experiment of coarse and then of fine ground malt and judge for himself.

ART. V.

_How to choose Malt._

Malt is chosen by its sweet smell, mellow taste, full flower, round body and thin skin. There are two kinds used, the pale and the brown--the pale is the best.

ART. VI.

_How to build a Malt kiln in every Distillery._

When setting up your stills, leave a space of about nine inches for a small furnace between the large ones, extend it to your chimney and carry up a funnel, there-from to the loft, then stop it--here build the kiln on the loft, about 4 or 5 feet square, the walls to be composed of single brick, 3 feet high--lay the bottom with brick, cover it with a plaster of mortar, to prevent the floor from taking fire. Turn the funnel of the chimney into, and extend it to the centre of the kiln, cover the top, leaving vent holes at the sides for the heat to escape thro'--Place on the top of the kiln, sheet iron or tin punched full of small holes, too small to admit the passage of malt; lay the malt on the top of the tin, when ready for drying. Put coals from under the still furnace into the small furnace leading to the kiln, which will heat the kiln and dry the malt above, by adding to or diminishing the quantity of coals, the heat may be increased or decreased, as may be found necessary. Malt for distilling ought to be dried without smoke.

ART. VII.

_Hops._

Give a preference to hops of a bright green colour, sweet smell, and have a gummy or clammy effect when rubbed between the hands or fingers.

SECTION V.

ARTICLE I.

_How to order and fill the Singling still when distilling Rye._

Scrape, clean, and grease the singling still, fill her up with beer, and keep a good fire under her, till she be warm enough to head, stirring her constantly with a broom, to prevent the grain from sticking to the bottom or sides, and burning, which it is very apt to do when the beer is cold, but when it comes to boil there is little danger, prevented by the motion of boiling; have the head washed clean--when she is ready for the head, clap it on and paste it; keep up a brisk fire, until she begins to drop from the worm, then put in the damper in the chimney, and if the fire be very strong, moderate it a little, by throwing ashes or water on it, to prevent her throwing the head, which she will be very apt to do if very full, and coming round under a strong fire, (should the head come, or be thrown off, the spirit remaining will scarcely be worth running off). When fairly round and running moderately, watch her for half an hour; after which, unless the fire is very strong all danger is over.

Should she happen to throw the head, it is the duty of the distiller to take and (wash the head and worm--the latter will be found full of stuff) clean, clap on the head, and paste it--but the moment the head is thrown off, the fire should be drowned out, and water thrown into the still to prevent her boiling over.

It is important that after every run, or rather before you commence a run, the distiller should carefully clean out the still, wipe the bottom dry, and grease her well, to prevent her from burning and singeing the liquor.

ART. II.

_Mode of managing the doubling Still when making Whiskey._

Let the doubling still be carefully cleaned and washed out, then be filled with singlings and low wines left from the run preceding, add thereto half a pint of salt and one quart of clean ashes, which will help to clear the whiskey, and a handful of Indian meal to prevent the still from leaking at the cock, or elsewhere--clean the head and worm, put on the head, paste it well; put fire under and bring her round slowly, and run the spirit off as slow as possible, and preserve the water in the cooling tub as cold as in your power.

Let the liquor as it runs from the worm pass thro' a flannel to prevent the overjuice from the copper, and the oil of the grain from mixing with the spirit. The first being poisonous, and the latter injurious to the liquor.

The doubling still cannot be run too slow for making good whiskey ... observe when the proof leaves the worm, that is when there is no proof on the liquor as it comes from the worm, if there be ten gallons in your doubling keg, if so, run out three more, which will make in all thirteen gallons first proof whiskey. If the proof leaves the worm at eight gallons, then run till eleven gallons and so on in proportion, to the larger or smaller quantity in your keg at the time of the ceasing of the proof.

ART. III.

_Observations on the advantages of making strong and good Whiskey with stalement, &c._

The distiller who makes whiskey for a market under the government of inspection laws, too weak, sustains a loss of a cent for each degree it may be under proof ... and the disadvantages are increased in proportion to the extent of land carriage. If a distance of seventy miles, the price of carriage per gallon will be about six cents, paying the same price for weak or strong ... not only the disadvantage of paying for the carriage of feints or water, but the loss in the casks, which tho' small apparently at first view, yet if nicely attended to, will amount in the course of the year to a sum of moment to every distiller or proprietor. To convey my ideas, or render a more compleat exposition of my impressions as to the actual loss on one waggon load (predicated on a distance of seventy miles land carriage) of first proof whiskey, and that nine degrees under proof. I give the following statement.

300 _gallons good first proof whiskey at_ 50 _cents_, $ 150 _haling at six cents_, 18 ________ $ 132 00