Chapter 3

I have directly ascertained that water thus filtered is deprived of all its germs. For this purpose I have added some of it (with the necessary precautions against introducing foreign organisms) to very changeable liquids, such as veal broth, blood, and milk, and have found that there was no alteration. Such water, then, is incapable of transmitting the germs of disease.

With an apparatus like the one here figured, and in which the filtering tube is eight inches in length by about one inch in diameter, about four and a half gallons of water per day may be obtained when the pressure is two atmospheres--the mean pressure in Mr. Pasteur's laboratory, where my experiments were made. Naturally, the discharge is greater or less according to the pressure. A discharge of three and a half to four and a half gallons of water seems to me to be sufficient for the needs of an ordinary household. For schools, hospitals, barracks, etc., it is easy to obtain the necessary volume of water by associating the tubes in series. The discharge will be multiplied by the number of tubes.

In the country, or in towns that have no water mains, it will be easy to devise an arrangement for giving the necessary pressure. An increase in the porosity of the filtering tube is not to be thought of, as this would allow very small germs to pass. This filter being a perfect one, we must expect to see it soil quickly. Filters that do not get foul are just the ones that do not filter. But with the arrangement that I have adopted the solid matters deposit upon the external surface of the filter, while the inner surface always remains perfectly clean. In order to clean the tube, it is only necessary to take it out and wash it vigorously. As the tube is entirely of porcelain, it may likewise be plunged into boiling water so as to destroy the germs that may have entered the sides or, better yet, it may be heated over a gas burner or in an ordinary oven. In this way all the organic matter will be burned, and the tube will resume its former porosity.--_M. Chamberland, La Nature._

* * * * *

SIMPLE DEVICES FOR DISTILLING WATER.

The alchemists dreamed and talked of that universal solvent which they so long and vainly endeavored to discover; still, for all this, not only the alchemist of old, but his more immediate successor, the chemist of to-day, has found no solvent so universal as water. No liquid has nearly so wide a range of dissolving powers, and, taking things all round, no liquid exercises so slight an action upon the bodies dissolved--evaporate the water away, and the dissolved substance is obtained in an unchanged condition; at any rate, this is the general rule.

The function of water in nature is essentially that of a solvent or a medium of circulation; it is not, in any sense, a food, yet without it no food can be assimilated by an animal. Without water the solid materials of the globe would be unable to come together so closely as to interchange their elements; and unless the temperatures were sufficiently high to establish an igneous fluidity, such as undoubtedly exists in the sun, there would be no circulation of matter to speak of, and the earth would be, as it were, locked up or dead.

When we look upon water as the nearest approach to a universal solvent that even the astute scientist of to-day has been able to discover, who can wonder that it is never found absolutely pure in nature? For wherever it accumulates it dissolves something from its surroundings. Still, in a rain-drop just formed we have very nearly pure water; but even this contains dissolved air to the extent of about one-fiftieth of its volume, and as the drop falls downward it takes up such impurities as may be floating in the atmosphere; so that if our rain-drop is falling immediately after a long drought, it becomes charged with nitrate or nitrite of ammonia and various organic matters--perhaps also the spores or germs of disease. Thus it will be seen that rain tends to wonderfully clear or wash the atmosphere, and we all know how much a first rain is appreciated as an air purifier, and how it carries down with it valuable food for plants. The rain-water, in percolating through or over the land, flows mainly toward the rivers, and in doing so it becomes more or less charged with mineral matter, lime salts and common salt being the chief of them; while some of that water which has penetrated more deeply into the earth takes up far more solid matter than is ordinarily found in river water. The bulk of this more or less impure water tends toward the ocean, taking with it its load of salt and lime. Constant evaporation, of course, takes place from the surface of the sea, so that the salt and lime accumulate, this latter being, however, ultimately deposited as shells, coral, and chalk, while nearly pure or naturally distilled water once more condenses in the form of clouds. This process, by which a constant supply of purified water is kept up in the natural economy, is imitated on a small scale when water is converted into steam by the action of heat, and this vapor is cooled so as to reproduce liquid water, the operation in question being known as distillation.

For this purpose an apparatus known as a still is required; and although by law one must pay an annual license fee for the right to use a still, it is not usual for the government authorities to enforce the law when a still is merely used for purifying water.

One of the best forms of still for the photographer to employ consists of a tin can or bottle in which the water is boiled, and to this a tin tube is adapted by means of a cork, one end of this tin tube terminating in a coil passing through a tub or other vessel of cold water. A gas burner, as shown, is a convenient source of heat, and in order to insure a complete condensation of the vapor, the water in the cooling tub must be changed now and again.

Sometimes the vapor is condensed by being allowed to play against the inside of a conical cover which is adapted to a saucepan, and is kept cool by the external application of cold water; and in this case the still takes the form represented by the subjoined diagrams; such compact and portable stills being largely employed in Ireland for the private manufacture of whisky.

It is scarcely necessary to say that the condensed water trickles down on the inside of the cone, and flows out at the spout.

An extemporized arrangement of a similar character may be made by passing a tobacco pipe through the side of a tin saucepan as shown below, and inverting the lid of the saucepan; if the lid is now kept cool by frequent changes of water inside it, and the pipe is properly adjusted so as to catch the drippings from the convex side of the lid, a considerable quantity of distilled water may be collected in an hour or so.

The proportion of solid impurities present in water as ordinarily met with is extremely variable: rain water which has been collected toward the end of a storm contains only a minute fraction of a grain per gallon, while river or spring water may contain from less than thirty grains per gallon or so and upward. Ordinary sea water generally contains from three to four per cent. of saline matter, but that of the Dead Sea contains nearly one-fourth of its weight of salts.

The three impurities of water which most interest the photographer are lime or magnesia salts, which give the so-called hardness; chlorides (as, for example, chloride of sodium or common salt), which throw down silver salts; and organic matter, which may overturn the balance of photographic operations by causing premature reduction of the sensitive silver compounds. To test for them is easy. Hardness is easily recognizable by washing one's hands in the water, the soap being curdled; but in many cases one must rather seek for a hard water than avoid it, as the tendency of gelatine plates to frill is far less in hard water than in soft water. It is, indeed, a common and useful practice to harden the water used for washing by adding half an ounce or an ounce of Epsom salts (sulphate of magnesia) to each bucket of water. Chlorides--chloride of sodium or common salt being that usually met with--may be detected by adding a drop or two of nitrate of silver to half a wineglassful of the water, a few drops of nitric acid being then added. A slight cloudiness indicates a trace of chlorides, and a decided milkiness shows the presence of a larger quantity. If it is wished to get a somewhat more definite idea of the amount, it is easy to make up a series of standards for comparison, by dissolving known weights of common salt in distilled or rain water, and testing samples of them side by side with the water to be examined.

Organic matters may be detected by adding a little nitrate of silver to the water, filtering off from any precipitate of chloride of silver, and exposing the clear liquid to sunlight; a clean stoppered bottle being the most convenient vessel to use. The extent to which a blackening takes place may be regarded as approximately proportionate to the amount of organic matter present.

Filtration on a small scale is not altogether a satisfactory mode of purifying water, as organic impurities often accumulate in the filter, and enter into active putrefaction when hot weather sets in.--_Photo. News._

* * * * *

IMPROVED FIRE-DAMP DETECTER.

According to the London _Mining Journal_, Mr. W.E. Garforth, of Normanton, has introduced an ingenious invention, the object of which is to detect fire-damp in collieries with the least possible degree of risk to those engaged in the work. Mr. Garforth's invention, which is illustrated in the diagram given below, consists in the use of a small India rubber hand ball, without a valve of any description; but by the ordinary action of compressing the ball, and then allowing it to expand, a sample of the suspected atmosphere is drawn from the roof, or any part of the mine, without the great risk which now attends the operation of testing for gas should the gauze of the lamp be defective. The sample thus obtained is then forced through a small protected tube on to the flame, when if gas is present it is shown by the well-known blue cap and elongated flame. From this description, and from the fact that the ball is so small that it can be carried in the coat pocket, or, if necessary, in the waistcoat pocket, it will be apparent what a valuable adjunct Mr. Garforth's invention will prove to the safety-lamp. It has been supposed by some persons that explosions have been caused by the fire-trier himself, but owing to his own death in most cases the cause has remained undiscovered. This danger will now be altogether avoided. It is well known that the favorite form of lamp with the firemen is the Davy, because it shows more readily the presence of small quantities of gas; but the Davy was some years ago condemned, and is now strictly prohibited in all Belgian and many English mines. Recent experience, gained by repeated experiments with costly apparatus, has resulted in not only proving the Davy and some other descriptions of lamps to be unsafe, but some of our Government Inspectors and our most experienced mining engineers go so far as to say that "no lamp in a strong current of explosive gas is safe unless protected by a tin shield."

If such is the case, Mr. Garforth seems to have struck the key-note when, in the recent paper read before the Midland Institute of Mining and Civil Engineers, and which we have now before us, he says: "It would seem from the foregoing remarks that in any existing safety-lamp where one qualification is increased another is proportionately reduced; so it is doubtful whether all the necessary requirements of sensitiveness, resistance to strong currents, satisfactory light, self-extinction, perfect combustion, etc., can ever be combined in one lamp."

The nearest approach to Mr. Garforth's invention which we have ever heard of is that of a workman at a colliery in the north of England, who, more than twenty years ago, to avoid the trouble of getting to the highest part of the roof, used a kind of air pump, seven or eight feet long, to extract the gas from the breaks; and some five years ago Mr. Jones, of Ebbw Vale, had a similar idea. It appears that these appliances were so cumbersome, besides requiring too great length or height for most mines, and necessitating the use of both hands, that they did not come into general use. The ideas, however, are totally different, and the causes which have most likely led to the invention of the ball and protected tube were probably never thought of until recently; indeed, Mr. Garforth writes that he has only learned about them since his paper was read before the Midland Institute, and some weeks after his patent was taken out.

No one, says Mr. Garforth, in his paper read before the Midland Institute, will, I presume, deny that the Davy is more sensitive than the tin shield lamp, inasmuch as in the former the surrounding atmosphere or explosive mixture has only one thickness of gauze to pass through, and that on a level with the flame; while the latter has a number of small holes and two or three thicknesses of gauze (according to the construction of the lamp), which the gas must penetrate before it reaches the flame. Moreover, the tin shield lamp, when inclined to one side, is extinguished (though not so easily as the Mueseler); and as the inlet holes are 6 inches from the top, it does not show a thin stratum of fire-damp near the roof as perceptibly as the Davy, which admits of being put in almost a horizontal position. Although the Davy lamp was, nearly fifty years ago, pronounced unsafe, by reason of its inability to resist an ordinary velocity of eight feet per second, yet it is still kept in use on account of its sensitiveness. Its advocates maintain that a mine can be kept safer by using the Davy, which detects small quantities of gas, and thereby shows the real state of the mine, than by a lamp which, though able to resist a greater velocity, is not so sensitive, and consequently is apt to deceive. Assuming the Davy lamp to be condemned (as it has already been in Belgium and in some English mines), the Stephenson and some of the more recently invented lamps pronounced unsafe, then if greater shielding is recommended the question is, what means have we for detecting small quantities of fire-damp?

It would seem from the foregoing remarks that in any existing safety-lamp, where one qualification is increased another is proportionately reduced; so it is doubtful whether all the necessary requirements of sensitiveness, resistance to strong currents, satisfactory light, self-extinction, perfect combustion, etc., can ever be combined in one lamp. The object of the present paper is to show that with the assistance of the fire-damp detecter, the tin shield, or any other description of lamp, is made as sensitive as the Davy, while its other advantages of resisting velocity, etc., are not in any way interfered with. As a proof of this I may mention that a deputy of experience recently visited a working place to make his inspection. He reported the stall to be free from gas, but when the manager and steward visited it with the detecter, which they applied to the roof (where it would have been difficult to put even a small Davy), it drew a sample of the atmosphere which, on being put to the test tube in the tin-shield lamp, at once showed the presence of fire-damp. Out of twenty-eight tests in a mine working a long-wall face the Davy showed gas only eleven times, while the detecter showed it in every case. The detecter, as will be perceived from the one exhibited, and the accompanying sectional drawing, consists simply of an oval-shaped India rubber ball, fitted with a mouthpiece. The diameter is about 2¼ inches by 3 inches, its weight is two ounces, and it is so small that it can be carried without any inconvenience in the coat or even in the waistcoat pocket. Its capacity is such that all the air within it may be expelled by the compression of one hand.

The mouthpiece is made to fit a tube in the bottom of the lamp, and when pressed against the India rubber ring on the ball-flange, a perfectly tight joint is made, which prevents the admission of any external air. The tube in the bottom of the lamp is carried within a short distance of the height of the wick-holder. It is covered at the upper end with gauze, besides being fitted with other thicknesses of gauze at certain distances within the tube; and if it be found desirable to further protect the flame against strong currents of air, a small valve may be placed at the inlet, as shown in the drawing. This valve is made of sufficient weight to resist the force of a strong current, and is only lifted from its seat by the pressure of the hand on the mouthpiece. It will be apparent from the small size and elasticity of the detecter that the test can easily be made with one hand, and when the ball is allowed to expand a vacuum is formed within it, and a sample of the atmosphere drawn from the breaks, cavities, or highest parts of the roof, or, of course, any portion of the mine. When the sample is forced through the tube near the flame, gas if present at once reveals itself by the elongation of the flame in the usual way, at the same time giving an additional proof by burning with a blue flame on the top of the test tube. If gas is not present, the distinction is easily seen by the flame keeping the same size, but burning with somewhat greater brightness, owing to the increased quality of oxygen forced upon it.

I venture to claim for this method of detecting fire-damp among other advantages: 1. The detecter, on account of its size, can be placed in a break in the roof where an ordinary lamp--even a small Davy--could not be put, and a purer sample of the suspected atmosphere is obtained than would be the case even a few inches below the level of the roof, 2. The obtaining and testing of a sample in the manner above described takes away the possibility of an explosion, which might be the result if a lamp with a defective gauze were placed in an explosive atmosphere. No one knows how many explosions have not been caused by the fire-trier himself. This will now be avoided. (Although lamps fitted with a tin shield will be subjected to the same strict examination as hitherto, still they do not admit of the same frequent inspection as those without shields, for in the latter case each workman can examine his own lamp as an extra precaution; whereas the examination of the tin shield lamps will rest entirely with the lamp man.) 3. The lamp can be kept in a pure atmosphere while the sample is obtained by the detecter, and at a greater height than the flame in a safety-lamp could be properly distinguished. The test can afterward be made in a safe place, at some distance from the explosive atmosphere; and, owing to the vacuum formed, the ball (without closing the mouthpiece) has been carried a mile or more without the gas escaping. 4. The detecter supplies a better knowledge of the condition of the working places, especially in breaks and cavities in the roof; which latter, with the help of a nozzle and staff, may be reached to a height of ten feet or more, by the detecter being pressed against the roof and sides, or by the use of a special form of detecter. 5. Being able at will to force the contents of the detecter on to the flame, the effects of an explosion inside the lamp need not be feared. (This danger being removed, admits, I think, of the glass cylinder being made of a larger diameter, whereby a better light is obtained; it may also be considered quite as strong, when used with the detecter, as a lamp with a small diameter, when the latter is placed in an explosive atmosphere.) 6. The use of the detecter will permit the further protection of the present tin shield lamp, by an extra thickness of gauze, if such addition is found advantageous in resisting an increased velocity. 7. In the Mueseler, Stephenson, and other lamps, where the flame is surrounded by glass, there is no means of using the wire for shot firing. The detecter tube, although protected by two thicknesses of gauze, admits of this being done by the use of a special form of valve turned by the mouthpiece of the detecter. The system of firing shots or using open lamps in the same pit where safety lamps are used is exceedingly objectionable; still, under certain conditions shots may be fired without danger. Whether safety lamps or candles are used, it is thought the use of the detecter will afford such a ready means of testing that more examinations will be made before firing a shot, thereby insuring greater safety. 8. In testing for gas with a safety lamp there is a fear of the light being extinguished, when the lamp is suddenly placed in a quantity of gas, or in endeavoring to get a very small light; this is especially the case with some kinds of lamps. With the detecter this is avoided, as a large flame can be used, which is considered by some a preferable means of testing for small quantities; and the test can be made without risk. Where gas is present in large quantities, the blue flame at the end of the test tube will be found a further proof. This latter result is produced by the slightest compression of the ball. (I need not point out the inconvenience and loss of time in having to travel a mile or more to relight.) As regards the use of the detecter with open lights, several of the foregoing advantages or modifications of them will apply. Instead of having to use the safety lamp as at present, it is thought that the working place will be more frequently examined, for a sample of the suspected atmosphere can be carried to a safe place and forced on to the naked light, when, if gas be present, it simply burns at the end of the mouthpiece like an ordinary gas jet. There are other advantages, such as examining the return airways without exposing the lamp, etc., which will be apparent, and become of more or less importance according to the conditions under which the tests are made.

In conclusion, I wish to paint out that the practice adopted at some collieries, of having all the men supplied with the most approved lamp (such as the Mueseler or tin shield lamp) is not a safe one. If the strength of a chain is only equal to the weakest link, it may be argued that the safety of a mine is only equal to that of the most careless man or most unsafe lamp in it. If, therefore, the deputies, whose duty it is to look for gas and travel the most dangerous parts of the mine, are obliged to use the Davy on account of its sensitiveness, may it not be said that, as their lamps are exposed equally with the workmen's to the high velocities of air, they are the weak links in the safety of the mine? For the reasons given, I venture to submit that the difficulties and dangers I have mentioned will be largely reduced, if not wholly overcome, by the use of the fire-damp detecter.

* * * * *

CAMERA ATTACHMENT FOR PAPER PHOTO NEGATIVES.

In computing the weight of the various items for a photographic tour, the glass almost invariably comes out at the head of the list, and the farther or longer the journey, so much more does the weight of the plates stand out pre-eminent; indeed, if one goes out on a trip with only three dozen half-plates, the glass will probably weigh nearly as much as camera, backs, and tripod, in spite of the stipulation with the maker to supply plates on "thin glass."