On the Construction of a Silvered Glass Telescope Fifteen and a half inches in aperture, and its use in celestial photography

Part 2

Chapter 23,997 wordsPublic domain

A short historical sketch of this telescope may not be uninteresting. In the summer of 1857, I visited Lord Rosse’s great reflector, at Parsonstown, and, in addition to an inspection of the machinery for grinding and polishing, had an opportunity of seeing several celestial objects through it. On returning home, in 1858, I determined to construct a similar, though smaller instrument; which, however, should be larger than any in America, and be especially adapted for photography. Accordingly, in September of that year, a 15 inch speculum was cast, and a machine to work it made. In 1860, the observatory was built, by the village carpenter, from my own designs, at my father’s country seat, and the telescope with its metal speculum mounted. This latter was, however, soon after abandoned, and silvered glass adopted. During 1861, the difficulties of grinding and polishing that are detailed in this account were met with, and the remedies for many of them ascertained. The experiments were conducted by the aid of three 15-1/2 inch disks of glass, together with a variety of smaller pieces. Three mirrors of the same focal length and aperture are almost essential, for it not infrequently happens that two in succession will be so similar, that a third is required for attempting an advance beyond them. One of these was made to acquire a parabolic figure, and bore a power of 1,000. The winter was devoted to perfecting the art of silvering, and to the study of special photographic processes. A large portion of 1862 was spent with a regiment in a campaign in Virginia, and but few photographs were produced till autumn, when sand clocks and clepsydras of several kinds having been made, the driving mechanism attained great excellence. During the winter, the art of local corrections was acquired, and two 15-1/2 inch mirrors, as well as two of 9 inches for the photographic enlarging apparatus, were completed. The greater part of 1863 has been occupied by lunar and planetary photography, and the enlargement of the small negatives obtained at the focus of the great reflector. Lunar negatives have been produced which have been magnified to 3 feet in diameter. I have also finished two mirrors 15-1/2 inches in aperture, suitable for a Herschelian telescope, that is, which can only converge oblique pencils to a focus free from aberration. This work has all been accomplished in the intervals of professional labor.

The details of the preceding operations are arranged as follows: §1. GRINDING AND POLISHING THE MIRRORS; §2. THE TELESCOPE MOUNTING; §3. THE CLOCK MOVEMENT; §4. THE OBSERVATORY; §5. THE PHOTOGRAPHIC LABORATORY; §6. THE PHOTOGRAPHIC ENLARGER.

§1. GRINDING AND POLISHING THE MIRRORS.

(1.) EXPERIMENTS ON A METAL SPECULUM.

My first 15 inch speculum was an alloy of copper and tin, in the proportions given by Lord Rosse. His general directions were closely followed, and the casting was very fine, free from pores, and of silvery whiteness. It was 2 inches thick, weighed 110 pounds, and was intended to be of 12 feet focal length. The grinding and polishing were conducted with the Rosse machine. Although a great amount of time was spent in various trials, extending over more than a year, a fine figure was never obtained--the principal obstacle to success being a tendency to polish in rings of different focal length. It must, however, be borne in mind that Lord Rosse had so thoroughly mastered the peculiarities of his machine as to produce with it the largest specula ever made and of very fine figure.

During these experiments there was occasion to grind out some imperfections, 8/100 of an inch deep, from the face of the metal. This operation was greatly assisted by stopping up the defects with a thick alcoholic solution of Canada balsam, and having made a rim of wax around the edge of the mirror, pouring on nitro-hydrochloric acid, which quickly corroded away the uncovered spaces. Subsequently an increase in focal length of 15 inches was accomplished, by attacking the edge zones of the surface with the acid in graduated depths.

An attempt also was made to assist the tedious grinding operation by including the grinder and mirror in a Voltaic circuit, making the speculum the positive pole. By decomposing acidulated water between it and the grinder, and thereby oxidizing the tin and copper of the speculum, the operation was much facilitated, but the battery surface required was too great for common use. If a sufficient intensity was given to the current, speculum metal was transferred without oxidation to the grinder, and deposited in thin layers upon it. It was proposed at one time to make use of this fact, and coat a mirror of brass with a layer of speculum metal by electrotyping. The gain in lightness would be considerable.

During the winter of 1860 the speculum was split into two pieces, by the expansion in freezing of a few drops of water that had found their way into the supporting case.

(2.) Silvering Glass.

At Sir John Herschel’s suggestion (given on the occasion of a visit that my father paid him in 1860), experiments were next commenced with silvered glass specula. These were described as possessing great capabilities for astronomical purposes. They reflect more than 90 per cent. of the light that fulls upon them, and only weigh one-eighth as much as specula of metal of equal aperture.

As no details of Steinheil’s or Foucault’s processes for silvering in the cold way were accessible at the time, trials extending at intervals over four months were made. A variety of reducing agents were used, and eventually good results obtained with milk sugar.

Soon after a description of the process resorted to by M. Foucault in his excellent experiments was procured. It consists in decomposing an alcoholic solution of ammonia and nitrate of silver by oil of cloves. The preparation of the solutions and putting them in a proper state of instability are very difficult, and the results by no means certain. The silver is apt to be soft and easily rubbed off, or of a leaden appearance. It is liable to become spotted from adherent particles of the solutions used in its preparation, and often when dissolved off a piece of glass with nitric acid leaves a reddish powder. Occasionally, however, the process gives excellent results.

In the winter of 1861, M. Cimeg published his method of silvering looking-glasses by tartrate of potash and soda (Rochelle salt). Since I have made modifications in it fitting the silver for being polished on the reverse side, I have never on any occasion failed to secure bright, hard, and in every respect, perfect films.

The operation, which in many details resembles that of M. Foucault, is divided into: 1st, cleaning the glass; 2d, preparing the solutions; 3d, warming the glass; 4th, immersion in the silver solution and stay there; 5th, polishing. It should be carried on in a room warmed to 70° F. at least. The description is for a 15-1/2 inch mirror.

1st. Clean the glass like a plate for collodion photography. Rub it thoroughly with nitric acid, and then wash it well in plenty of water, and set it on edge on filtering paper to dry. Then cover it with a mixture of alcohol and prepared chalk, and allow evaporation to take place. Rub it in succession with many pieces of cotton flannel. This leaves the surface almost chemically clean. Lately, instead of chalk I have used plain uniodized collodion, and polished with a freshly-washed piece of cotton flannel, as soon as the film had become semi-solid.

2d. Dissolve 560 grains of Rochelle salt in two or three ounces of water and filter. Dissolve 800 grains of nitrate of silver in four ounces of water. Take an ounce of strong ammonia of commerce, and add nitrate solution to it until a brown precipitate remains undissolved. Then add more ammonia and again nitrate of silver solution. This alternate addition is to be carefully continued until the silver solution is exhausted, when some of the brown precipitate should remain in suspension. The mixture then contains an undissolved excess of oxide of silver. Filter. Just before using, mix with the Rochelle salt solution, and add water enough to make 22 ounces.

The vessel in which the silvering is to be performed may be a circular dish (Fig. 1) of ordinary tinplate, 16-1/2 inches in diameter, with a flat bottom and perpendicular sides one inch high, and coated inside with a mixture of beeswax and rosin (equal parts), At opposite ends of one diameter two narrow pieces of wood, _a a′_, 1/8 of an inch thick, are cemented. They are to keep the face of the mirror from the bottom of the vessel, and permit of a rocking motion being given to the glass. Before using such a vessel, it is necessary to touch any cracks that may have formed in the wax with a hot poker. A spirit lamp causes bubbles and holes through to the tin. The vessel too must always, especially if partly silvered, be cleaned with nitric acid and water, and left filled with cold water till needed. Instead of the above, India-rubber baths have been occasionally used.

3d. In order to secure fine and hard deposits in the shortest time and with weak solutions, it is desirable, though not necessary, to warm the glass slightly. This is best done by putting it in a tub or other suitably sized vessel, and pouring in water enough to cover the glass. Then hot water is gradually stirred in, till the mixture reaches 100° F. It is also advantageous to place the vessels containing the ingredients for the silvering solution in the same bath for a short time.

4th. On taking the glass out of the warm water, carry it to the silvering vessel--into which an assistant has just previously poured the mixed silvering solution--and immediately immerse it face downwards, dipping in first one edge and then quickly letting down the other till the face is horizontal. The back of course is not covered with the fluid. The same precautions are necessary to avoid streaks in silvering as in the case of putting a collodion plate in the bath. Place the whole apparatus before a window. Keep up a slow rocking motion of the glass, and watch for the appearance of the bright silver film. The solution quickly turns brown, and the silver soon after appears, usually in from three to five minutes. Leave the mirror in the liquid about six times as long. At the expiration of the twenty minutes or half hour lift it out, and look through it at some very bright object. If the object is scarcely visible, the silver surface must then be washed with plenty of water, and set on edge on bibulous paper to dry. If, on the contrary, it is too thin, put it quickly back, and leave it until thick enough. When polished the silver ought, if held between the eye and the sun, to show his disk of a light blue tint. On coming out of the bath the metallic surface should have a rosy golden color by reflected light.

5th. When the mirror is thoroughly dry, and no drops of water remain about the edges, lay it upon its back on a thoroughly dusted table. Take a piece of the softest thin buckskin, and stuff it loosely with cotton to make a rubber. Avoid using the edge pieces of a skin, as they are always hard and contain nodules of lime.

Go gently over the whole silver surface with this rubber in circular strokes, in order to commence the removal of the rosy golden film, and to condense the silver. Then having put some very fine rouge on a piece of buckskin laid flat on the table, impregnate the rubber with it. The best stroke for polishing is a motion in small circles, at times going gradually round on the mirror, at times across on the various chords (Fig. 2). At the end of an hour of continuous gentle rubbing, with occasional touches on the flat rouged skin, the surface will be polished so as to be perfectly black in oblique positions, and, with even moderate care, scratchless. The process is like a burnishing. Put the rubber carefully away for another occasion.

The thickness of the silver thus deposited is about 1/200,000 of an inch. Gold leaf, when equally transparent, is estimated at the same fraction. The actual value of the amount on a 15-1/2 inch mirror is not quite a cent--the weight being less than 4 grains (239 milligrammes on one occasion when the silver was unusually thick), if the directions above given are followed.

Variations in thickness of this film of silver on various parts of the face of the mirror are consequently only small fractions of 1/200,000 of an inch, and are therefore of no optical moment whatever. If a glass has been properly silvered, and shows the sun of the same color and intensity through all parts of its surface, the most delicate optical tests will certainly fail to indicate any difference in figure between the silver and the glass underneath. The faintest peculiarities of local surface seen on the glass by the method of M. Foucault, will be reproduced on the silver.

The durability of these silver films varies, depending on the circumstances under which they are placed, and the method of preparation. Sulphuretted hydrogen tarnishes them quickly. Drops of water may split the silver off. Under certain circumstances, too, minute fissures will spread all over the surface of the silver, and it will apparently lose its adhesion to the glass. This phenomenon seems to be connected with a continued exposure to dampness, and is avoided by grinding the edge of the concave mirror flat, and keeping it covered when not in use with a sheet of flat plate glass. Heat seems to have no prejudicial effect, though it might have been supposed that the difference in expansibility would have overcome the mutual adhesion.

Generally silvered mirrors are very enduring, and will bear polishing repeatedly, if previously dried by heat. I have some which have been used as diagonal reflectors in the Newtonian, and have been exposed during a large part of the day to the heat of the sun concentrated by the 15-1/2 inch mirror. These small mirrors are never covered, and yet the one now in the telescope has been there a year, and has had the dusty film--like that which accumulates on glass--polished off it a dozen times.

In order to guard against tarnishing, experiments were at first made in gilding silver films, but were abandoned when found to be unnecessary. A partial conversion of the silver film into a golden one, when it will resist sulphuretted hydrogen, can be accomplished as follows: Take three grains of hyposulphite of soda, and dissolve it in an ounce of water. Add to it slowly a solution in water of one grain of chloride of gold. A lemon yellow liquid results, which eventually becomes clear. Immerse the silvered glass in it for twenty-four hours. An exchange will take place, and the film become yellowish. I have a piece of glass prepared in this way which remains unhurt in a box, where other pieces of plain silvered glass have changed some to yellow, some to blue, from exposure to coal gas.

I have also used silvered glass plates for daguerreotyping. They iodize beautifully if freshly polished, and owing probably to the absence of the usual copper alloy of silver plating, take impressions with very short exposures. The resulting picture has a rosy warmth, rarely seen in ordinary daguerreotypes. The only precaution necessary is in fixing to use an alcoholic solution of cyanide of potassium, instead of hyposulphite of soda dissolved in water. The latter has a tendency to split up the silver. The subsequent washing must be with diluted common alcohol.

Pictures obtained by this method will bear high magnifying powers without showing granulation. Unfortunately the exposure required for them in the telescope is six times as great as for a sensitive wet collodion, though the iodizing be carried to a lemon yellow, the bromizing to a rose red, and the plate be returned to the iodine.

(3.) GRINDING AND POLISHING GLASS.

Some of the facts stated in the following paragraphs, the result of numerous experiments, may not be new to practical opticians. I have had, however, to polish with my own hands more than a hundred mirrors of various sizes, from 19 inches to 1/4 of an inch in diameter, and to experience very frequent failures for three years, before succeeding in producing large surfaces with certainty and quickly. It is well nigh impossible to obtain from opticians the practical minutiæ which are essential, and which they conceal even from each other. The long continued researches of Lord Rosse, Mr. Lassell, and M. Foucault are full of the most valuable facts, and have been of continual use.

The subject is divided into: a. The Peculiarities of Glass; b. Emery and Rouge; c. Tools of Iron, Lead and Pitch; d. Methods of Examining Surfaces; e. Machines.

a. _Peculiarities of Glass._

_Effects of Pressure._--It is generally supposed that glass is possessed of the power of resistance to compression and rigidity in a very marked manner. In the course of these experiments it has appeared that a sheet of it, even when very thick, can with difficulty be set on edge without bending so much as to be optically worthless. Fortunately in every disk of glass that I have tried, there is one diameter on either end of which it may stand without harm.

In examining lately various works on astronomy and optics, it appears that the same difficulty has been found not only in glass but also in speculum metal. Short used always to mark on the edge of the large mirrors of his Gregorian telescopes the point which should be placed uppermost, in case they were removed from their cells. In achromatics the image is very sensibly changed in sharpness if the flint and crown are not in the best positions; and Mr. Airy, in mounting the Northumberland telescope, had to arrange the means for turning the lenses on their common axis, until the finest image was attained. In no account, however, have I found a critical statement of the exact nature of the deformation, the observers merely remarking that in some positions of the object glass there was a sharper image than in others.

Before I appreciated the facts now to be mentioned, many fine mirrors were condemned to be re-polished, which, had they been properly set in their mountings, would have operated excellently.

In attempting to ascertain the nature of deformations by pressure, many changes were made in the position of the disk of glass, and in the kind of support. Some square mirrors, too, were ground and polished. As an example of the final results, the following case is presented: A 15-1/2 inch unsilvered mirror 1-1/4 inch thick was set with its best diameter perpendicular, the axis of the mirror being horizontal (Fig. 8). The image of a pin-hole illuminated by a lamp was then observed to be single, sharply defined, and with interference rings surrounding it as at _a_, Fig. 3. On turning the glass 90 degrees, that is one quarter way round, its axis still pointing in the same direction, it could hardly be realized that the same concave surface was converging the rays. The image was separated into two of about equal intensity, as at _b_, with a wing of light going out above and below from the junction. Inside and outside of the focal plane the cone of rays had an elliptical section, the major axis being horizontal inside, and perpendicular outside. Turning the mirror still more round the image gradually improved, until the original diameter was perpendicular again--the end that had been the uppermost now being the lowest. A similar series of changes occurred in supporting the glass on various parts of the other semicircle. It might be supposed that irregularities on the edge of the glass disk, or in the supporting arc would account for the phenomena. But two facts dispose of the former of these hypotheses: in the first place if the glass be turned exactly half way round, the character of the image is unchanged, and it is not to be believed that in many different mirrors this could occur by chance coincidence. In the second place, one of these mirrors has been carefully examined after being ground and polished three times in succession, and on each occasion required the same diameter to be perpendicular. As to the second hypothesis no material difference is observed whether the supporting arc below be large or small, nor when it is replaced by a thin semicircle of tinplate lined with cotton wool.

I am led to believe that this peculiarity results from the structural arrangement of the glass. The specimens that have served for these experiments have probably been subjected to a rolling operation when in a plastic state, in order to be reduced to a uniform thickness. Optical glass, which may be made by softening down irregular fragments into moulds at a temperature below that of fusion, may have the same difficulty, but whether it has a diameter of minimum compression can only be determined by experiment. Why speculum metal should have the same property might be ascertained by a critical examination of the process of casting, and the effect of the position of the openings in the mould for the entrance of the molten metal.

_Effects of Heat._--The preceding changes in glass when isolated appear very simple, and their remedy, to keep the proper diameter perpendicular, is so obvious that it may seem surprising that they should have given origin to any embarrassment. In fact it is now desirable to have a disk in which they are well marked. But in practice they are complicated in the most trying manner with variations produced by heat pervading the various parts of the glass unequally. The following case illustrates the effects of heat:--

A 15-1/2 inch mirror, which was giving at its centre of curvature a very fine image (_a_, Fig. 4) of an illuminated pin-hole, was heated at the edge by placing the right hand on the back of the mirror, at one end of the horizontal diameter. In a few seconds an arc of light came out from the image as at _b′_, and on putting the left hand on the other extremity of the same diameter the appearance _c′_ was that of two arcs of light crossing each other, and having an image at each intersection. The mirror did not recover its original condition in ten minutes. Another person on a subsequent occasion touching the ends of the perpendicular diameter at the same time that the horizontal were warmed, caused the image _d′_ to become somewhat like two of _c′_, put at right angles to each other. A little distance outside the focus the complementary appearances, _b_, _c_, _d_, were found.

By unsymmetrical warming still more remarkable forms emerged in succession, some of which were more like certain nebulæ with their milky light, than any regular geometrical figure.

If the glass had, after one of these experiments, been immediately put on the polishing machine and re-polished, the changes in surface would to a certain extent have become permanent, as in Chinese specula, and the mirror would have required either re-grinding or prolonged polishing to get rid of them. This occurred unfortunately very frequently in the earlier stages of this series of experiments, and gave origin on one occasion to a surface which could only show the image of a pin-hole as a lozenge (_b_, Fig. 5), with an image at each angle inside the focus, and as an image a with four wings outside.